Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Aminobenzoic Acid → 3-[(Pyridin-4-yl)amino]benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Aminobenzoic Acid | HCID 7419 | — |
| 반응물 | 4-Chloropyridine | HCID 12288 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 3-[(Pyridin-4-yl)amino]benzoic acid | HCID 13712475 | — |
반응 단계
3-(4-Pyridinylamino)benzoic acid was prepared from 41.1 g of m-aminobenzoic acid and 34.0 g of 4-chloropyridine in 110 ml of acetic acid, heated at reflux for 6 hours. With a work-up procedure similar to that of Example 33, there was obtained 48.5 g of product, m.p. 172°-180° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04610991 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-dd186632b4854b4aa65d99b84bc932a3 |
| 출처 메모 | uspto-grants-1986_09 |