Ammonia → 3-(4-Pyridinylamino)benzamide

HRID 64896

반응식

HRID 64896 반응식
[N:1]1[CH:6]=[CH:5][C:4]([NH:7][C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11](O)=[O:12])=[CH:3][CH:2]=1.[NH3:17]>>[N:1]1[CH:6]=[CH:5][C:4]([NH:7][C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11]([NH2:17])=[O:12])=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 222AmmoniaHCID 137124753-[(Pyridin-4-yl)amino]benzoic acid

생성물 1

HCID 137124763-(4-Pyridinylamino)benzamide수율 50%

실험 절차

3-(4-Pyridinylamino)benzamide was prepared from 3-(4-pyridinylamino)benzoic acid and ammonia according to the procedure of Example 48, part (b), and was obtained in 50% yield as a colorless powder, m.p. 201°-203° C. when recrystallized from methanol.

후처리

  1. customwas obtained in 50% yield as a colorless powder, m.p. 201°-203° C. when
  2. customrecrystallized from methanol

출처 및 근거

ORD 기록
ord-97b00eea7a994df3861f4e4a6b98738e
출처 데이터셋
uspto-grants-1986_09
특허 번호
US04610991

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