Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-bromobutanimide → 2-(2,2-Dichlorovinyl)-benzyl bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 2-(2,2-Dichlorovinyl)-toluene | HCID 13713127 | — |
| 용매 | 1,1,1-Trichloroethane | HCID 6278 | — |
| 생성물 | 2-(2,2-Dichlorovinyl)-benzyl bromide | HCID 13713128 | — |
반응 단계
211 g (1.13 moles) of 2-(2,2-dichlorovinyl)-toluene, 251 g (1.41 moles) of N-bromosuccinimide and 2 g of azoisobutyronitrile in 1300 ml of dry 1,1,1-trichloroethane are refluxed, an additional 1 g of azoisobutyronitrile is added to the reaction mixture after one hour, and heating is continued for a further hour.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04611010 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-760ebf0ea2264cd3a5e2e56550388425 |
| 출처 메모 | uspto-grants-1986_09 |