Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylpyridine → 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylpyridine | HCID 7975 | — |
| 반응물 | 2-(4-Chlorophenyl)-3-methylbutanoyl chloride | HCID 4178001 | — |
| 반응물 | 2-(2,2-Dichlorovinyl)-benzaldehyde | HCID 13713131 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate | HCID 13713135 | — |
반응 단계
2.8 g (0.012 mole) of 2-(4-chlorophenyl)-isovaleryl chloride in 50 ml of absolute toluene are introduced into 1.2 g (0.013 mole) of -picoline and 3.2 g (0.015 mole) of 2-(2,2-dichlorovinyl)-benzaldehyde in a conical flask at room temperature, while stirring. After 30 minutes, the mixture is filtered under suction over silica gel, and washing is carried out with toluene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04611010 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-0f238b4ef3e5448f8833fd83cb856d4f |
| 출처 메모 | uspto-grants-1986_09 |