Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Malonate → Diethyl pentafluorobenzylmalonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Malonate | HCID 7761 | — |
| 반응물 | Pentafluorobenzaldehyde | HCID 69558 | — |
| 생성물 | Diethyl pentafluorobenzylmalonate | HCID 88651511 | 69% |
반응 단계
9 g of pentafluorobenzaldehyde are condensed on 7 g of diethyl malonate in accordance with the process described in Organic Synthesis vol. III, page 377. 10 g (69%) of diethyl pentafluorobenzylmalonate are obtained which is hydrogenated at ordinary pressure in the presence of palladium on charcoal into diethyl pentafluorobenzylmalonate (92%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04738803 |
| 출처 데이터셋 | uspto-grants-1988_04 |
| ORD ID | ord-16b1b55501134601a9cbffcc03de0787 |
| 출처 메모 | uspto-grants-1988_04 |