Cesium fluoride → Allyl Oxalofluoride

HRID 649255

반응식

HRID 649255 반응식
[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

참가 물질

3

반응물 2

HCID 25953Cesium fluorideHCID 3018516Allyl chlorooxoacetate

생성물 1

HCID 14153244Allyl Oxalofluoride

실험 절차

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

후처리

  1. distillationto twice distilled title product, b.p. 48°-50° C./35 mm
  2. custom124°-126° C. (atmospheric pressure)

출처 및 근거

ORD 기록
ord-e0232b6b3e3e495ca8bd281a4b73c66e
출처 데이터셋
uspto-grants-1988_04
특허 번호
US04739047

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