Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Di-tert-butyl-4-mercaptophenol → 1,1-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)methane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| 반응물 | 3,5-Di-tert-butyl-4-hydroxybenzaldehyde | HCID 73219 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1,1-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)-1-(3,5-di-tert-butyl-4-hydroxyphenyl)methane | HCID 13710008 | 87% |
반응 단계
The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 11.72 grams of 3,5-di-tert-butyl-4-hydroxybenzaldehyde and 150 ml of methyl alcohol. Trituration with methyl alcohol gives 30 grams (87% yield) of white crystals, mp 175°-177° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04611023 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-36a37f1261b44d6ab252646882ffa253 |
| 출처 메모 | uspto-grants-1986_09 |