Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzaldehyde → alpha,alpha-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)toluene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzaldehyde | HCID 240 | — |
| 반응물 | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | alpha,alpha-Bis(3,5-di-tert-butyl-4-hydroxyphenylthio)toluene | HCID 13710010 | 66.3% |
반응 단계
The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 5.31 grams of benzaldehyde, and 150 ml of methyl alcohol. The product is triturated with methyl alcohol to give 18.74 grams (66% yield) of white crystals, mp 122°-124° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04611023 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-b62ff9936c7f41b984ee1d508e7d4ac6 |
| 출처 메모 | uspto-grants-1986_09 |