Methanol → HCID 13710011, 화합물

HRID 64940

반응식

[C:1]([C:5]1[CH:10]=[C:9]([SH:11])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]=1[OH:16])([CH3:4])([CH3:3])[CH3:2].[CH2:17]([CH:19]([CH2:22][CH2:23][CH2:24][CH3:25])[CH:20]=O)[CH3:18].[CH3:26][OH:27]>>[C:1]([C:5]1[CH:10]=[C:9]([S:11][CH:20]([S:11][C:9]2[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:6]([OH:16])=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH:10]=2)[CH:19]([CH2:17][CH3:18])[CH2:22][CH2:23][CH2:24][CH3:25])[CH:8]=[C:7]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:26]=1[OH:27])([CH3:4])([CH3:3])[CH3:2]

참가 물질

반응물 3

HCID 887Methanol

HCID 312412-Ethylhexanal

HCID 703702,6-Di-tert-butyl-4-mercaptophenol

생성물 1

HCID 13710011HCID 13710011, 화합물

실험 절차

The procedure of Example 1 is repeated using 23.84 grams of 2,6-di-tert-butyl-4-mercaptophenol, 6.41 grams of 2-ethylhexanal, and 150 ml of methyl alcohol. The product is purified by dry-column chromatography to give 10.29 grams of a clear syrup.

후처리

customThe product is purified by dry-column chromatography

출처 및 근거

ORD 기록: ord-6fd87e6b59f448079a43bff64df13065
출처 데이터셋: uspto-grants-1986_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04611023

연결된 노트

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