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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 649608생성일: 2026년 10월 24일

Diethyl Ether → Lytron 810

https://huagongshe.com/ko/reaction/649608

반응식

참여 물질

역할이름HCID투입량
반응물Diethyl EtherHCID 3283—
반응물Alpha-MethylstyreneHCID 7407—
반응물Maleic AnhydrideHCID 7923—
용매Methyl Ethyl KetoneHCID 6569—
생성물Lytron 810HCID 6270745.4%

반응 조건

온도60 °C

반응 단계

In 200 ml of methyl ethyl ketone were dissolved 18.14 g of maleic anhydride and 21.86 g of α-methylstyrene, and to the solution was added 1.82 g of azobisisobutylnitrile (AIBN). The resulting mixture was heated at 60° C. for 7 hours under nitrogen atmosphere for performing polymerization. The reaction solution was then dropwise added to 500 ml of ethyl ether under stirring to precipitate a polymer. Thus precipitated polymer was collected by filtration and purified by repeating twice the THF dissolution-ethyl ether precipitation procedure described in Example 1. Thus purified polymer was dried under vacuum at 100° C. for 24 hours to give 17.0 g of a maleic anhydride-styrene copolymer. It was confiremed by elementary analysis that the copolymerization ratio was approximately 1:1. Mn was 11,730.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04740561
출처 데이터셋uspto-grants-1988_04
ORD IDord-62cc2b624ec0476c8a8c832a2bb87f20
출처 메모uspto-grants-1988_04