반응식
N[C:2]1[CH:7]=CC=C[CH:3]=1.C=CC.[NH2:11][C:12]1[C:13]([CH3:18])=[CH:14][CH:15]=[CH:16][CH:17]=1>>[CH3:18][C:13]1[CH:14]=[CH:15][CH:16]=[C:17]([CH:2]([CH3:7])[CH3:3])[C:12]=1[NH2:11]참가 물질
4
실험 절차
2-Methyl-6-isopropyl aniline was prepared by the method of Example 2 using an H-Y zeolite catalyst for the condensation of aniline and propylene. The ortho-toluidine and propylene were fed to the reactor in a 1:5 molar ratio and at an LHSV of 0.25 based on o-toluidine. The reaction was conducted at 250° C. and 861 psig. The effluent product stream was analyzed by gas chromatography. Conversion of o-toluidine was 81.5%.
후처리
- customwas conducted at 250° C.
출처 및 근거
- ORD 기록
- ord-ee4902f425e34214aaeafb0b03e5c094
- 출처 데이터셋
- uspto-grants-1988_04
- 특허 번호
- US04740620
연결된 노트
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