Propylene → 2-Fluoro-6-isopropylaniline
반응식
[CH2:1]=[CH:2][CH3:3].[F:4][C:5]1[CH:11]=[CH:10][CH:9]=[CH:8][C:6]=1[NH2:7]>>[F:4][C:5]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:2]([CH3:3])[CH3:1])[C:6]=1[NH2:7]참가 물질
3
실험 절차
2-fluoro-6-isopropyl aniline was prepared by the method of Example 2 using an H-Y zeolite catalyst for the condensation of 2-aniline and propylene. In this reaction 2-fluoroaniline and propylene were fed to a reactor in a 1:5 mole ratio and LHSV of 0.25 based on 2-fluoroaniline. The reaction was conducted at 255° C. and 879 psig. The effluent product stream was analyzed by gas chromatography. Conversion of 2-fluoroaniline was 71.2%.
후처리
- customwere fed to a reactor in a 1
- customwas conducted at 255° C.
출처 및 근거
- ORD 기록
- ord-d89cdea7afc641629ad73de353885a55
- 출처 데이터셋
- uspto-grants-1988_04
- 특허 번호
- US04740620
반응 노트
불러오는 중…