Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 9-(1,3-Di-n-octanoyloxy-2-propoxymethyl)guanine | HCID 136332159 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 9-(1,3-di-n-octanoyloxy-2 propoxymethyl)guanine HCl | HCID 136332160 | — |
반응 단계
A twofold stoichiometric excess of 3% hydrogen chloride in methanol is added to a solution of 1.0 g. of 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine in 20 ml methanol. Diethyl ether is added until precipitation is complete. The product is filtered, washed with ether, air dried and recrystallized to give 9-(1,3-di-n-octanoyloxy-2-propoxymethyl)guanine hydrochloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04612314 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-44085480c8624b88860ea735b0070417 |
| 출처 메모 | uspto-grants-1986_09 |