Triethylamine → HCID 69686974, 화합물

HRID 651169

반응식

HRID 651169 반응식
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[NH:9][NH2:10].[C:11]([O:16][CH2:17][CH3:18])(=O)[C:12]([CH3:14])=[O:13].C(N(CC)CC)C>C(O)C>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[NH:9][N:10]=[C:11]([O:16][CH2:17][CH3:18])[C:12](=[O:13])[CH3:14]

참가 물질

5

반응물 3

HCID 8471TriethylamineHCID 12041Ethyl pyruvateHCID 408929(2,4-Dichlorophenyl)hydrazine

생성물 1

HCID 69686974HCID 69686974, 화합물수율 98%

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of 2,4-dichlorophenylhydrazine (1.0 g, 4.7 mmol), ethyl pyruvate (0.53 mL, 4.7 mmol), triethylamine (0.65 mL, 4.7 mmol) and ethanol (5 mL) was heated at reflux overnight. The solvent was evaporated and the residue taken up in chloroform. The solution was washed with water and brine and dried over magnesium sulfate and concentrated, leaving an oil (1.1 g, 98%).

후처리

  1. temperaturewas heated
  2. temperatureat reflux overnight
  3. customThe solvent was evaporated
  4. washThe solution was washed with water and brine
  5. dry with materialdried over magnesium sulfate
  6. concentrationconcentrated

출처 및 근거

ORD 기록
ord-ceb1d970f5d1424dafb2778a7069dc57
출처 데이터셋
uspto-grants-2001_08
특허 번호
US06277877B1

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