참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzoyl chloride | HCID 7412 | — |
| 반응물 | Carbonic acid, di-2-propen-1-yl ester | HCID 84764 | — |
| 촉매 | Zincchloride | HCID 3007855 | — |
| 생성물 | Allyl benzoate | HCID 11406 | 82% |
반응 단계
In a glass reactor benzoyl chloride (7.03 g, 0.05 mole), diallyl carbonate (7.1 g, 0.05 mole) and zinc chloride (0.136 g, 0.001 mole) were combined. The reacinitiated at room temperature. After heating at 60° C. for 3 hours and heating at 80° C. for an additional 3 hours, the reaction was discontinued. Distillation gave 6.65 g (78 percent yield) of allyl benzoate which was identified by nuclear magnetic resonance spectroscopy.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04612386 |
|---|
| 출처 데이터셋 | uspto-grants-1986_09 |
|---|
| ORD ID | ord-39ac0fe3490b4b4ca1802b534a76f6ac |
|---|
| 출처 메모 | uspto-grants-1986_09 |
|---|
