Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-(Chloromethyl)-1,1'-biphenyl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 3-Biphenylmethanol | HCID 603556 | — |
| 생성물 | 3-(Chloromethyl)-1,1'-biphenyl | HCID 15480892 | — |
반응 단계
A solution of 50 mg of 3-hydroxymethylbiphenyl in 1.5 mL thionyl chloride was heated at reflux temperature for 4 hr, cooled to room temperature and the solvent removed by evaporation under reduced pressure to yield 45 mg of 3-chloromethylbiphenyl which was used in the next step without further purification or characterization.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06281359B1 |
| 출처 데이터셋 | uspto-grants-2001_08 |
| ORD ID | ord-4187c7e7eb114d3eba0842f23595041d |
| 출처 메모 | uspto-grants-2001_08 |