Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → N-[4-[14-(Trimethylsilyl)tetradecylamino]benzoyl)glycine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Ethyl 4-[14-(trimethylsilyl)tetradecylamino]hippurate | HCID 20198242 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-[4-[14-(Trimethylsilyl)tetradecylamino]benzoyl)glycine | HCID 20198286 | — |
반응 단계
A mixture of 12.5 g. of ethyl 4-[14-(trimethylsilyl)tetradecylamino]hippurate, 55 ml. of 1N sodium hydroxide solutions and 50 ml. of ethanol is stirred at ambient temperature for 2 hours and then partially evaporated. The aqueous solution is washed with diethyl ether, acidified with 6N hydrochloric acid, and filtered. The solid is dried in vacuo and recrystallized to yield the product as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04670421 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-51d702da3ab148408fdf35a26672fdea |
| 출처 메모 | uspto-grants-1987_06 |