Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine hydrate (1:1) → HCID 178480237, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 반응물 | 4-(2-Fluorobenzoyl)-1-methylpiperidine | HCID 13180317 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178480237 | HCID 178480237 | 23.7% |
반응 단계
An autoclave was charged with 10.0 g of 4-(2-fluorobenzoyl)-1-methylpiperidine and 14 ml of hydrazine hydrate. The reaction was heated at 150° for 20 hrs, cooled, and poured into water. The resultant solid was collected. The solid was recrystallized twice from toluene to yield 2.4 g (23.7%) of product, mp 168°-170° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04670447 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-cdd33599bdaa477e8b872b2930c887a2 |
| 출처 메모 | uspto-grants-1987_06 |