Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(3-Bromopropoxy)-3-nitrobenzene → 3-(3-Bromopropoxy)-aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(3-Bromopropoxy)-3-nitrobenzene | HCID 7172301 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 3-(3-Bromopropoxy)-aniline | HCID 459256 | — |
반응 단계
1 g of Raney nickel is added to a solution of 4 g of 3-(3-bromopropoxy)-nitrobenzene in 40 ml of tetrahydrofuran and the starting substance is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. Evaporation of the filtrate gives 3-(3-bromopropoxy)-aniline as a colourless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04670604 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-0bc7908018df4e4c82b06dbd11cc14b4 |
| 출처 메모 | uspto-grants-1987_06 |