Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4-Chlorophenyl)-2-butyn-1-ol → (Z)-1-(4-chlorophenyl)-2-buten-1-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4-Chlorophenyl)-2-butyn-1-ol | HCID 20188339 | — |
| 촉매 | Lindlars catalyst | HCID 131709914 | — |
| 생성물 | (Z)-1-(4-chlorophenyl)-2-buten-1-ol | HCID 67901371 | — |
반응 단계
Under nitrogen, hydrogenate a mixture of 10 g (0.055 mole) of 1-(4-chlorophenyl)-2-butyn-1-ol and 0.6 g Lindlar catalyst. Following the reaction vic NMR the reaction is complete in about two days. The hydrogenation is stopped and the reaction stirred under N2 at room temperature overnight. Filter off the catalysts, wash with methylene chloride combine the filtrate and evaporate to yield the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613609 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-1ba35f007e7240af90d3407e16dabfe8 |
| 출처 메모 | uspto-grants-1986_09 |