1-Methylimidazole → HCID 178480862, 화합물

HRID 65251노트

반응식

HRID 65251 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11]Cl)=[CH:4][CH:3]=1.[CH3:13][N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1>>[Cl-:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N+:16]2[CH:17]=[CH:18][N:14]([CH3:13])[CH:15]=2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 13901-MethylimidazoleHCID 200827321-Chloro-4-(4-chlorobutyl)benzene

생성물 1

HCID 178480862HCID 178480862, 화합물

실험 절차

Combine 6.1 g (0.03 mole) 1-chloro-4-(4-chlorobutyl)benzene with 2.5 g (0.03 mole) 1-methyl-1H-imidazole and heat at 120° C., following the course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5). At the completion of the reaction, cool and triturate with ether, collect the solid and recrystallize from 50 ml hot acetone to obtain the title compound.

후처리

  1. customthe course of the reaction by thin-layer chromatography on silica gel (methanol: 1M sodium chloride, 95:5)
  2. customAt the completion of the reaction
  3. temperaturecool
  4. customtriturate with ether
  5. customcollect the solid
  6. customrecrystallize from 50 ml hot acetone

출처 및 근거

ORD 기록
ord-789f015a518643958156a7ed367e7d7e
출처 데이터셋
uspto-grants-1986_09
특허 번호
US04613609

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