Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → HCID 178480903, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | N-[4-(1-Hydroxy-2-(1H-imidazol-1-yl)ethyl]phenyl]methanesulfonamide | HCID 13763390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178480903 | HCID 178480903 | — |
반응 단계
Heat a solution of 4.0 g (14.2 mmole) of (±)-N-[4-[1-hydroxy-2-(1H-imidazol-1-yl)ethyl]phenyl]methanesulfonamide, 2 ml (32.1 mmole) of iodomethane and 50 ml methanol in a glass pressure tube to 80° C. for 24 hours. Remove the solvent in vacuo. Crystallize the residue from acetone. Recrystallize from acetone to provide the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613609 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-30a8001166504f31b5d5e17ea568ca6b |
| 출처 메모 | uspto-grants-1986_09 |