Aniline → HCID 18931494, 화합물

HRID 652834노트

반응식

[N+:1]([C:4]1[C:5]([N+:13]([O-:15])=[O:14])=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7](Cl)=[O:8])([O-:3])=[O:2].[NH2:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[N+:1]([C:4]1[C:5]([N+:13]([O-:15])=[O:14])=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7]([NH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:8])([O-:3])=[O:2]

참가 물질

반응물 2

HCID 6115Aniline

HCID 11413586Dinitrobenzoyl chloride

생성물 1

HCID 18931494HCID 18931494, 화합물

실험 절차

Dinitrobenzoyl chloride is caused to react with aniline so as to give dinitrobenzanilide. Thereafter, the resulting product is caused to react with Ar--N(R)2 and oxyphosphorous chloride and to the resulting product concentrated hydrochloric acid is added to prepare a compound having the formula: ##STR5##

출처 및 근거

ORD 기록: ord-fd2a7a569840467c836697f1a1801e28
출처 데이터셋: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04673773

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