Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexane → 2-(3-Hydroxyphenyl)-2-oxoacetaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | 3-Hydroxyacetophenone | HCID 8487 | — |
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-(3-Hydroxyphenyl)-2-oxoacetaldehyde | HCID 12910875 | — |
반응 단계
Using 1:1 hexane:ethyl acetate as eluant, the method of Preparation 68 was employed to convert 3-hydroxyacetophenone (15.0 g., 0.11 mol) to present title product, 7.4 g.; 1H-nmr (DMSO-d6) 7.09 (m, 2H), 7.43 (m, 3H), 9.75 (br m, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04675186 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-02355845f5ff415e811e6659c2b78d5c |
| 출처 메모 | uspto-grants-1987_06 |