Dipotassium tetrachloroplatinate → Platinous chloride

HRID 653083

반응식

HRID 653083 반응식
Cl.Cl.[C:3]1([CH2:9][NH2:10])([CH2:7][NH2:8])[CH2:6][CH2:5][CH2:4]1.C([O-])(=O)C.[Na+].[Cl:16][Pt-2:17](Cl)(Cl)[Cl:18].[K+].[K+]>O>[C:3]1([CH2:9][NH2:10])([CH2:7][NH2:8])[CH2:6][CH2:5][CH2:4]1.[Pt:17]([Cl:18])[Cl:16]

참가 물질

6

반응물 3

HCID 61440Dipotassium tetrachloroplatinateHCID 517045Sodium AcetateHCID 202036281,1-Bis(aminomethyl)cyclobutane dihydrochloride

생성물 2

HCID 2770Platinous chlorideHCID 4328361,1-Cyclobutanedimethanamine

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A solution of 1.87 g of the above amine in 30 ml of water was treated with 1.64 g of solid sodium acetate followed by 4.15 g of potassium tetrachloroplatinate. The mixture was stirred overnight and filtered. The filtrate was concentrated, giving as a solid 1,1-cyclobutanedimethanamine, compound with platinum chloride.

후처리

  1. filtrationfiltered
  2. concentrationThe filtrate was concentrated

출처 및 근거

ORD 기록
ord-e8ec9817642b46d08a31487737b3a61d
출처 데이터셋
uspto-grants-1987_06
특허 번호
US04675336

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