N,N-Diethyl-1,3-propanediamine → HCID 13531622, 화합물

HRID 653094노트

반응식

HRID 653094 반응식
Br[CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[O:10][C:9]([N+:11]([O-:13])=[O:12])=[C:8]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:7]=2[CH:20]=1.[CH2:21]([N:23]([CH2:26][CH2:27][CH2:28][NH2:29])[CH2:24][CH3:25])[CH3:22]>C(O)C>[CH2:21]([N:23]([CH2:26][CH2:27][CH2:28][NH:29][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[O:10][C:9]([N+:11]([O-:13])=[O:12])=[C:8]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:7]=2[CH:20]=1)[CH2:24][CH3:25])[CH3:22]

참가 물질

4

반응물 2

HCID 61011N,N-Diethyl-1,3-propanediamineHCID 13531604HCID 13531604, 화합물

생성물 1

HCID 13531622HCID 13531622, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Using the method of Example 1, 5-bromomethyl-2-nitro-3-phenylbenzofuran is reacted with 3-(N,N-diethylamino)propylamine in ethanol to provide light tan crystals of 5-[3-(N,N-diethylamino)propylaminomethyl]-2-nitro-3-phenylbenzofuran dihydrochloridemonohydrate, m.p. 143°-150° C., having the structure

출처 및 근거

ORD 기록
ord-fef420c66c204a47a5dcfc98cdb8e468
출처 데이터셋
uspto-grants-1987_06
특허 번호
US04675320

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