Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Gallic Acid → Octyl Gallate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Gallic Acid | HCID 370 | — |
| 반응물 | 1-Octanol | HCID 957 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Octyl Gallate | HCID 61253 | 75% |
반응 단계
A mixture of 30 g of tara (about 0.1 mole of bound gallic acid), 120 g (0.95 mole) of n-octanol and 3 g of anhydrous sulfuric acid was heated at 140° C. for 7 hours with continuous removal of the water of reaction, after which the mixture was washed neutral with water and then evaporated down to give the crude n-octyl gallate in the form of an oil. The purity of the product was 65% and the yield was 75%, calculated as pure ester.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613683 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-e22881c9711f41c493927cfd24f41066 |
| 출처 메모 | uspto-grants-1986_09 |