Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methyl-3-buten-1-ol → 3-Methyl-3-butenyl 2-methylisocrotonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methyl-3-buten-1-ol | HCID 12988 | — |
| 반응물 | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| 반응물 | Dioctyltin laurate | HCID 22292224 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 3-Methyl-3-butenyl 2-methylisocrotonate | HCID 16205381 | — |
반응 단계
A mixture of 20.0 g. of methyl angelate, 22.65 g. of 3-methyl-3-butenyl alcohol, 100 ml. of toluene and 0.8 g. of dioctyltin laurate was reacted under the same conditions as in Example 6. The reaction mixture was subjected to single distillation to obtain 39.5 g. of a distillate boiling at 104° C. (32 mmHg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613680 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-af7ccfea57244031a639864f8090c451 |
| 출처 메모 | uspto-grants-1986_09 |