Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Hexenol → 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Hexenol | HCID 5281167 | — |
| 반응물 | Methyl (2Z)-2-methyl-2-butenoate | HCID 5356352 | — |
| 반응물 | Dioctyltin laurate | HCID 22292224 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-Butenoic acid, 2-methyl-, (3Z)-3-hexenyl ester, (2Z)- | HCID 16220109 | — |
반응 단계
A mixture of 20.0 g. of methyl angelate, 26.34 g. of (Z)-3-hexenyl alcohol, 100 ml. of toluene and 1.2 g. of dioctyltin laurate was placed in a 300 ml. glass flask, which was equipped with a Soxhlet extractor filled on the top with molecular sieve 4A and a reflux cooler.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613680 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-86d99ad2c96d423794886a4f3cc76510 |
| 출처 메모 | uspto-grants-1986_09 |