Chlorosulfonic acid → HCID 20195206, 화합물

HRID 653205노트

반응식

HRID 653205 반응식
[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][S:9](=[O:12])(=[O:11])[CH:8]=[CH:7][C:6]=2[CH:13]=1.[Cl:14][S:15](O)(=[O:17])=[O:16]>>[Br:1][C:2]1[CH:3]=[C:4]([S:15]([Cl:14])(=[O:17])=[O:16])[C:5]2[O:10][S:9](=[O:11])(=[O:12])[CH:8]=[CH:7][C:6]=2[CH:13]=1

참가 물질

3

반응물 2

HCID 24638Chlorosulfonic acidHCID 20195196HCID 20195196, 화합물

생성물 1

HCID 20195206HCID 20195206, 화합물

실험 절차

6.0 g of 6-bromo-2,2-dioxo-1,2-benzoxathiine and 22.0 g of chlorosulfonic acid are heated for 1 hour to 60° C. The mixture is then poured into ice-water. The precipitated 6-bromo-8-chlorosulfonyl-2,2-dioxo-1,2-benzoxathiine is isolated, washed with water and dried.

출처 및 근거

ORD 기록
ord-c73707c1accc42ee853b1b8a31b0568c
출처 데이터셋
uspto-grants-1987_06
특허 번호
US04675417

반응 노트

불러오는 중…