Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Acifluorfen sodium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Acifluorfen | HCID 44073 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Acifluorfen sodium | HCID 44072 | 105.4% |
반응 단계
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04613360 |
| 출처 데이터셋 | uspto-grants-1986_09 |
| ORD ID | ord-9e9b4f013e6e41fe8d4ab299c0212c3e |
| 출처 메모 | uspto-grants-1986_09 |