Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl Acetate → 1-(4-Aminophenyl)-3-n-butyl-3-azabicyclo[3.1.1]heptane-2,4-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 반응물 | 3-n-Butyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione | HCID 20027825 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-(4-Aminophenyl)-3-n-butyl-3-azabicyclo[3.1.1]heptane-2,4-dione | HCID 20027835 | — |
반응 단계
In a manner analogous to that described in Example 1, 2.08 g of 3-n-butyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione in 60 ml of ethanol are hydrogenated in the presence of 0.15 g of palladium-on-carbon and worked up. Melting point 178°-179° (from ethyl acetate).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04677129 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-f42a7228885d4602b39d28f643c4ef82 |
| 출처 메모 | uspto-grants-1987_06 |