Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluoroaniline → 4'-Fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluoroaniline | HCID 9731 | — |
| 반응물 | 5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid | HCID 227638 | — |
| 생성물 | 4'-Fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide | HCID 19760311 | 60.7% |
반응 단계
In a manner analogous to Example 1, 2 g of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalene-carboxylic acid and 1 g of 4-fluoroaniline were used to obtain 1.7 g of 4'-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide in colorless crystals. m.p. 163° C.-165° C. (from ethyl acetate/hexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05128470 |
| 출처 데이터셋 | uspto-grants-1992_07 |
| ORD ID | ord-8686e89e6f324c5c9d4bff1bfd4590c3 |
| 출처 메모 | uspto-grants-1992_07 |