1-Methoxy-4-nitro-3-(2-nitroethenyl)-2-(phenylmethoxy)benzene → HCID 18962537, 화합물

HRID 654381노트

반응식

HRID 654381 반응식
C(OC1C2OC=2C=C([N+]([O-])=O)C=1C=C[N+]([O-])=O)C1C=CC=CC=1.[CH2:24]([O:31][C:32]1[C:42]([O:43][CH3:44])=[CH:41][CH:40]=[C:39]([N+:45]([O-])=O)[C:33]=1[CH:34]=[CH:35][N+]([O-])=O)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[CH2:24]([O:31][C:32]1[C:42]([O:43][CH3:44])=[CH:41][CH:40]=[C:39]2[C:33]=1[CH:34]=[CH:35][NH:45]2)[C:25]1[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=1

참가 물질

3

반응물 2

HCID 538011151-Methoxy-4-nitro-3-(2-nitroethenyl)-2-(phenylmethoxy)benzeneHCID 86745996HCID 86745996, 화합물

생성물 1

HCID 18962537HCID 18962537, 화합물수율 86%

실험 절차

This compound is obtained according to the operating method described in Example 1c, in which the 2-benzyloxy-3-epoxy-6,β-dinitrostyrene is replaced with 2-benzyloxy-3-methoxy-6,β-dinitrostyrene. A white powder (yield=86%, m.p.=83°-84° C.) is obtained.

후처리

  1. customThis compound is obtained

출처 및 근거

ORD 기록
ord-8c607d35fcff421595538fb49d6da6b3
출처 데이터셋
uspto-grants-1992_07
특허 번호
US05131911

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