참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | — |
반응 단계
A mixture of 80.6 g of 5-chloro-2-nitrobenzoic acid and 58.2 ml of thionyl chloride is heated at 90° C. for 2 hours. The excess thionyl chloride is then distilled off in vacuo. 87.1 g of 5-chloro-2-nitrobenzoyl chloride are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05132314 |
|---|
| 출처 데이터셋 | uspto-grants-1992_07 |
|---|
| ORD ID | ord-a77377dc679e46d883508eddd15de74a |
|---|
| 출처 메모 | uspto-grants-1992_07 |
|---|
