2-Bromomethylnaphthalene → 3-Methoxy-4-(naphth-2-ylmethoxy)bromobenzene

HRID 654823노트

반응식

HRID 654823 반응식
Br[CH2:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1.[Br:13][C:14]1[CH:19]=[CH:18][C:17]([OH:20])=[C:16]([O:21][CH3:22])[CH:15]=1>>[CH3:22][O:21][C:16]1[CH:15]=[C:14]([Br:13])[CH:19]=[CH:18][C:17]=1[O:20][CH2:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1

참가 물질

3

반응물 2

HCID 703202-BromomethylnaphthaleneHCID 2622344-Bromo-2-methoxyphenol

생성물 1

HCID 200806073-Methoxy-4-(naphth-2-ylmethoxy)bromobenzene수율 62%

실험 절차

Using the procedure described in Example 1, 2-bromomethylnaphthalene was reacted with 4-bromo-2-methoxyphenol to give 3-methoxy-4-(naphth-2-ylmethoxy)bromobenzene in 62% yield, m.p. 108° C.

출처 및 근거

ORD 기록
ord-1baa5dd3d37b4175bada2aecc2d67e09
출처 데이터셋
uspto-grants-1992_07
특허 번호
US05134148

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