1,1'-Carbonyldiimidazole → 5-Methyloxazolo[4,5-b]pyridin-2(3H)-one

HRID 655309

반응식

HRID 655309 반응식
[NH2:1][C:2]1[C:7]([OH:8])=[CH:6][CH:5]=[C:4]([CH3:9])[N:3]=1.[C:10](N1C=CN=C1)(N1C=CN=C1)=[O:11]>>[CH3:9][C:4]1[N:3]=[C:2]2[NH:1][C:10](=[O:11])[O:8][C:7]2=[CH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 682631,1'-CarbonyldiimidazoleHCID 885002-Amino-6-methylpyridin-3-ol

생성물 1

HCID 100120755-Methyloxazolo[4,5-b]pyridin-2(3H)-one

실험 절차

Reaction of 2-amino-6-methylpyridin-3-ol with CDI (carbonyldiimidazole) in a corresponding manner to Example 1.2 gives the desired product; ESI: 151 (M+H), Rt=1.58 min (method B).

출처 및 근거

ORD 기록
ord-92cadd072a9947ba9cc51852f3894439
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08071593B2

연결된 노트

불러오는 중…