Water → Silver behenate

HRID 65548

반응식

HRID 65548 반응식
[C:1]([OH:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].O.[N+]([O-])([O-])=O.[Ag+:30]>C1C=CC=CC=1>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Ag+:30]

참가 물질

5

반응물 3

HCID 962Water2회HCID 8215Docosanoic AcidHCID 24470Silver Nitrate

생성물 1

HCID 164971Silver behenate

시약·촉매·용매 1

HCID 241Benzene용매

실험 절차

3.4 g of behenic acid was dissolved in 100 ml of benzene at 60° C., and the temperature of this solution was adjusted to 60° C. 100 ml of water was added to the above solution with stirring to form an emulsion. 100 ml of an aqueous solution of silver ammonium complex, which was prepared by adding aqueous to about 80 ml of an aqueous solution containing 1.7 g of silver nitrate, and then adding water to the aqueous solution to make the total volume one liter, was then added to the above emulsion. Crystallites of silver behenate were obtained.

후처리

  1. customwas adjusted to 60° C
  2. customto form an emulsion
  3. additionwas then added to the above emulsion

출처 및 근거

ORD 기록
ord-bea4512df7a544c7832af1c2098a4279
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04128428

연결된 노트

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