참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 2-Methyl-1-pentene | HCID 12986 | — |
| 반응물 | 4-Mercaptophenol | HCID 240147 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 4-(Hexylthio)phenol | HCID 20086310 | — |
반응 단계
A 4-(hexylthio)phenol was prepared as follows. In a one liter flask equipped with thermometer, stirring rod and water condenser was added 126 grams of 4-mercaptophenol and 7 grams of toluenesulfonic acid. The flask contents were heated to 60° C. and 93 grams of 2-methyl-1-pentene were added over a fifty minute period. The flask contents were neutralized with 9 grams of Na2CO3 in aqueous solution and decanted. The reaction product was stripped to a pot temperature of 80° C. at 20 millimeters of mercury. It weighed 216 grams.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04128530 |
|---|
| 출처 데이터셋 | uspto-grants-1978_12 |
|---|
| ORD ID | ord-ab70397f3e6949cf95fb20215605e801 |
|---|
| 출처 메모 | uspto-grants-1978_12 |
|---|
