참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | N-Methylolacrylamide | HCID 13543 | — |
| 반응물 | Lauryl acrylate | HCID 75084 | — |
| 촉매 | Benzoyl Peroxide | HCID 7187 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | N-hydroxymethyl acrylamide dodecyl acrylate | HCID 86736188 | 430.5% |
반응 단계
10.1 gm (0.1 mole) of N-hydroxymethyl acrylamide and 144 gm (0.6 mole) of dodecyl acrylate were dissolved in 360 gm of methyl ethyl ketone. To the solution obtained were added 3.1 gm of dibenzoyl peroxide as a catalyst. The reaction mixture was maintained for 5 hours under stirring at a temperature of 80° C. After the reaction was completed, the solvent was distilled off and the reaction product washed several times with methanol. 147 gm (95% of theory) of N-hydroxymethyl acrylamide/dodecyl acrylate copolymer (1:6 molar ratio) were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04128634 |
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| 출처 데이터셋 | uspto-grants-1978_12 |
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| ORD ID | ord-c9f8f0cc0f7d41979aea8df5c5aeb86b |
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| 출처 메모 | uspto-grants-1978_12 |
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