Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenacyl bromide → alpha-(4-Chloro-2-naphthoxy)acetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenacyl bromide | HCID 6259 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Chloro-1-naphthol | HCID 11787 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | alpha-(4-Chloro-2-naphthoxy)acetophenone | HCID 20563338 | — |
반응 단계
The product of step A is reacted with α-bromoacetophenone in benzene in the presence of potassium carbonate using the method of Example 1, step A, to provide white crystals of α-(4-chloro-2-naphthoxy)acetophenone after recrystallization from a dichloromethane-petroleum ether mixture.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04128659 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-bf48fa7d40fa410cb77be9c23de72d02 |
| 출처 메모 | uspto-grants-1978_12 |