Orotic Acid → Dicreatine orotate

HRID 657440

반응식

HRID 657440 반응식
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

참가 물질

4

반응물 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

생성물 1

HCID 131724698Dicreatine orotate

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Under room temperature 298 grams of creatine monohydrate is slowly added to 2.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with ethanol. After drying 410 grams of Dicreatine orotate is obtained.

후처리

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 410 grams of Dicreatine orotate
  5. customis obtained

출처 및 근거

ORD 기록
ord-bf3c6f5643184be7a9652d70df81c39a
출처 데이터셋
uspto-grants-2011_12
특허 번호
USRE043029E1

연결된 노트

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