Orotic Acid → Tricreatine orotate

HRID 657441

반응식

HRID 657441 반응식
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1>C(O)C>[C:11]([OH:21])(=[O:20])[C:12]1[NH:19][C:17](=[O:18])[NH:16][C:14](=[O:15])[CH:13]=1.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

참가 물질

4

반응물 2

HCID 967Orotic AcidHCID 80116Creatine Monohydrate

생성물 1

HCID 11444210Tricreatine orotate

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Under room temperature 447 grams of creatine monohydrate is slowly added to 3.5 liters of ethanol under agitation and stirring for 30 minutes. Then 156 grams of orotic acid is slowly added to the mixture during continuous stirring for 4 hours under room temperature. Finally filtration is utilized to remove the solvent and clean the residue with alcohol. After drying 555 grams of Tricreatine orotate is obtained.

후처리

  1. stirringduring continuous stirring for 4 hours under room temperature
  2. filtrationFinally filtration
  3. customto remove the solvent
  4. dry with materialAfter drying 555 grams of Tricreatine orotate
  5. customis obtained

출처 및 근거

ORD 기록
ord-9e2a2e1f8b6146c28c4ae7c7957b50e8
출처 데이터셋
uspto-grants-2011_12
특허 번호
USRE043029E1

연결된 노트

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