Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine → HCID 178483234, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-(((2-Aminoethyl)thio)methyl)-N,N-dimethyl-2-furanmethanamine | HCID 162203 | — |
| 반응물 | N-Nitro-S-methylisothiourea | HCID 135927615 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178483234 | HCID 178483234 | — |
반응 단계
A solution of 2-[[[5-(dimethylamino)methyl-2-furanyl]methyl]thio]ethanamine (2.14 g) and S-methyl-N-nitroisothiourea (1.5 g) in ethanol (10 ml) was heated to 40° for 5 mins. The resulting precipitate was filtered and recrystallised from ethyl acetate and petroleum ether b.p. 80°-100° to give N-[2-[[[5-(dimethylamino)methyl-2-furanyl]methyl]thio]ethyl]-N'-nitroguanidine m.p. 103°-104°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04128658 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-4db50c9413fa4078abfda28ae4674ee7 |
| 출처 메모 | uspto-grants-1978_12 |