Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-((Dimethylamino)methyl)-2-furanmethanol → Ranisen
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-((Dimethylamino)methyl)-2-furanmethanol | HCID 84906 | — |
| 반응물 | N-(2-Mercaptoethyl)-N'-methyl-2-nitro-1,1-ethenediamine | HCID 181798 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Potassium Carbonate | HCID 11430 | — |
| 생성물 | Ranisen | HCID 5039 | — |
반응 단계
N-(2-Mercaptoethyl)-N'-methyl-2-nitro-1,1-ethenediamine (354 mg) in concentrated hydrochloric acid (2 ml) was added dropwise to 5-(dimethylamino)methyl-2-furanmethanol (428 mg) at 0°. After standing at 0° for 7 days the reaction was diluted with water (3 ml), excess potassium carbonate was added and the solid extracted with ethyl acetate (50 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04128658 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-19209aada948472496e2dc6b9871a0e4 |
| 출처 메모 | uspto-grants-1978_12 |