Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Cyclohexen-1-one, 2,5,6-trimethyl- → 2,3,6-Trimethylphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Cyclohexen-1-one, 2,5,6-trimethyl- | HCID 89264 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 2,3,6-Trimethylphenol | HCID 17016 | 96% |
반응 단계
1000 g of 2,5,6-trimethyl-2-cyclohexen-1-one is passed per hour per liter of catalyst at atmospheric pressure through an externally heated tube having a capacity of 250 cm3 and filled with a palladium/silica gel catalyst (0.2% by weight of palladium), the temperature being 300° C. The yield is 96% of 2,3,6-trimethylphenol. 4% of starting material is recovered and returned to the reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04128728 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-6c0e52ac2c3e41c5a1a9b2712864ce14 |
| 출처 메모 | uspto-grants-1978_12 |