Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyladipate → Disodium adipate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyladipate | HCID 12329 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Disodium adipate | HCID 24073 | — |
반응 단계
17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04129520 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-af3c1eef92454c249d5f397014b710cf |
| 출처 메모 | uspto-grants-1978_12 |