Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diazomethane → Methyl 3,5-Dibromobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diazomethane | HCID 9550 | — |
| 반응물 | Benzoic acid, 3,5-dibromo- | HCID 12063 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Methyl 3,5-Dibromobenzoate | HCID 621923 | — |
반응 단계
To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08076359B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-c9c0b78b58ea4da49f17993ef5b5aaae |
| 출처 메모 | uspto-grants-2011_12 |