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Hexamethylenetetramine → Molybdenum hexamethylenetetramine

HRID 65826
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HRID 65826 반응식
[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3.O[Mo:12](O)(=O)=O.[NH4+].[NH4+].[O-][Mo]([O-])(=O)=O>O>[Mo:12].[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3
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참가 물질

5

반응물 3

HCID 4101HexamethylenetetramineHCID 61578Diammonium molybdateHCID 82208Molybdic acid

생성물 1

HCID 131710930Molybdenum hexamethylenetetramine

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

Hexamethylenetetramine molybdate having a 2/1 molybdenum/hexamethylenetetramine molar ratio was prepared as follows. 10 grams of hexamethylenetetramine was dissolved in 100 ml water heated near reflux temperature. 24.01 grams of commercial, so-called "molybdic acid" (actually at least one ammonium molybdate) was dissolved in 169 ml water heated to reflux temperature. The first solution was added to the second solution.

후처리

  1. temperatureheated
  2. temperaturenear reflux temperature
  3. temperatureheated
  4. temperatureto reflux temperature
  5. additionThe first solution was added to the second solution

출처 및 근거

ORD 기록
ord-242010b0e43b497ba711f280db016fe8
출처 데이터셋
uspto-grants-1978_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04129540

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