Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Chloroethyl vinyl ether → 1-Cyclohexyl-4-[2-(ethenyloxy)ethoxy]benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Chloroethyl vinyl ether | HCID 8074 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4-Cyclohexylphenol | HCID 14327 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 촉매 | Tetrabutylammonium Bromide | HCID 74236 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-Cyclohexyl-4-[2-(ethenyloxy)ethoxy]benzene | HCID 22011687 | — |
반응 단계
In 300 ml of toluene, 83.1 g (0.5 mol) of p-cyclohexylphenol was dissolved and subsequently, 150 g of 2-chloroethyl vinyl ether, 25 g of sodium hydroxide, 5 g of tetrabutylammonium bromide and 60 g of triethylamine were added and reacted at 120° C. for 5 hours. The reaction solution was washed with water, excess chloroethyl vinyl ether and toluene were distilled off and the obtained oil was purified by distillation under reduced pressure to obtain 4-cyclohexylphenoxyethyl vinyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07083892B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-2bff57c9dfc8421dbe6ed3b86c52a9d7 |
| 출처 메모 | uspto-grants-2006_08 |